题干

为测定某三价铁配合物(化学式表示为Ka[Feb(C2O4)c]·xH2O)的组成,做了如下实验:

步骤1:称取1.9640g Ka[Feb(C2O4)c]·xH2O晶体,配制成250.00mL溶液.

步骤2:取所配溶液25.00mL于锥形瓶中,加入1mol/LH2SO45.0mL,加热到70~85℃,用0.01000mol/LKMnO4溶液滴定至终点(5C2O42-+2MnO4-+16H+=10CO2↑+2Mn2++8H2O),消耗KMnO4溶液48.00mL。

步骤3:向反应后的溶液中加入一定量锌粉。加热至黄色恰好消失,过滤,洗涤,将过滤及洗涤所得溶液收集到锥形瓶中,此时溶液仍呈酸性。

步骤4:继续用0.01000mol/LKMnO4溶液滴定步骤3所得溶液至终点,消耗KMnO4溶液8.00mL。

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