题干

氮化镁是一种应用范围非常广泛的无机化合物,它可用于制备高硬度、高热导、抗腐蚀、抗磨损和耐高温的其它元素的氮化物,制备特殊的陶瓷材料等.某校化学研究小组用镁与氮气反应制备氮化镁(Mg3N2),并用实验方法测定氮化镁的纯度.

I.制备氮化镁

【查阅资料】

①(NH42SO4+2NaNO2 Δ__ 2N2↑+Na2SO4+4H2O,该反应为放热反应.

②饱和硫酸亚铁溶液能吸收氧气;稀硫酸能吸收氨气.

③在常温下或温度不高的条件下镁几乎与水不反应.

【实验】

制备氮化镁的装置示意图如图1

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